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Melting ceramic Al2O3 powder by electron beam powder bed fusion
Mid Sweden University, Faculty of Science, Technology and Media, Department of Engineering, Mathematics, and Science Education (2023-). (SportsTech Research Center)ORCID iD: 0000-0003-3218-875X
Mid Sweden University, Faculty of Science, Technology and Media, Department of Engineering, Mathematics, and Science Education (2023-). (SportsTech Research Center)
Universitat Politècnica de Catalunya, Spain.
2024 (English)In: Progress in Additive Manufacturing, ISSN 2363-9512, E-ISSN 2363-9520, Vol. 9, p. 1523-1535Article in journal (Refereed) Published
Abstract [en]

Electron beam powder bed fusion (PBF-EB) is a known metal additive manufacturing (AM) technology. Processing non-conducting powders such as ceramics has so far been considered as not feasible because of the inherent problems with Coulomb repulsion due to insufficient electrical conductivity. In this study, a method for functionalizing ceramic powder is proposed where particles are electroless coated by a ~ 1 µm Ni layer to decrease the surface resistivity. The feasibility of the suggested approach is tested on Al2O3 powder, and the results show that the coated ceramic powder has a decreased surface resistivity, which enables processing by PBF-EB. Heating and melting parameters were investigated and samples were manufactured at ~ 1600 °C. Sintered and melted powders were analyzed by microscopy and micromechanically tested by nanoindentation. Calculations, visual observation and SEM–EDX suggest that the Ni coating is evaporated during the process, which suggests that the process could be feasible for the manufacturing of pure ceramic parts.

Place, publisher, year, edition, pages
Springer, 2024. Vol. 9, p. 1523-1535
National Category
Other Materials Engineering
Identifiers
URN: urn:nbn:se:miun:diva-50773DOI: 10.1007/s40964-024-00601-4ISI: 001198017900001Scopus ID: 2-s2.0-85189612765OAI: oai:DiVA.org:miun-50773DiVA, id: diva2:1841052
Available from: 2024-11-12 Created: 2024-02-27 Last updated: 2026-03-12Bibliographically approved
In thesis
1. Material Development for Electron Beam-based Powder Bed Fusion
Open this publication in new window or tab >>Material Development for Electron Beam-based Powder Bed Fusion
2024 (English)Licentiate thesis, comprehensive summary (Other academic)
Abstract [en]

Electron beam powder bed fusion (PBF-EB) is an additivemanufacturing (AM) method based on layer-by-layer melting of apowder bed. The technology is industrialized in certain applicationsbut still considered as immature and is not as widely used as laserbeam-based systems (PBF-LB). PBF-EB can offer several benefits overPBF-LB such as process cleanliness, thermal efficiency, fast beam speed,higher power and energy transfer, low residual stresses in built partsand a good signal environment for process monitoring. This can beadded on top of the general benefits of AM such as geometricalfreedom, manufacturing efficiency, easy design revisions, short leadtimes and so on. This suggests that PBF-EB holds potential as atechnology for the sustainable production of materials andcomponents. This thesis investigates how PBF-EB can be furtherdeveloped to create new and unique materials features. This isachieved by introducing innovative methods for material processingand by further developing the PBF-EB process itself. The thesisintroduces a charge-free heating method for PBF-EB and the resultssuggest an enhanced processability of difficult-to-process materialsand powders. A method for building multi-materials in PBF-EB isintroduced and demonstrated by the manufacturing of direct andlamellar transitions between different alloys. Methods for processmonitoring and powder bed resistivity evaluation are proposed andxiidemonstrated. It is concluded that the results presented in this thesisenabled new PBF-EB processing modes, increased the knowledge ofthe process, and introduced a new material group by demonstratingthat ceramics can be processed at high temperatures (~1600C).

Place, publisher, year, edition, pages
Sundsvall: Mid Sweden University, 2024. p. 109
Series
Mid Sweden University licentiate thesis, ISSN 1652-8948 ; 202
Keywords
Additive manufacturing, Electron beam, Powder bed fusion, EBM, PBF-EB, PBF-EB/M, PBF-EB/C, Process development, Material development, Ti-6Al-4V, 316L, V4E, Al2O3
National Category
Mechanical Engineering
Identifiers
urn:nbn:se:miun:diva-50762 (URN)978-91-89786-54-7 (ISBN)
Presentation
2024-03-26, Q221, Akademigatan 1, Östersund, 09:00 (English)
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Supervisors
Note

Vid tidpunkten för framläggningen av avhandlingen var följande delarbeten opublicerade: delarbete 2 och delarbete 4 (inskickat).

At the time of the defence the following papers were unpublished: paper 2 and paper 4 (submitted).

Available from: 2024-02-27 Created: 2024-02-26 Last updated: 2025-09-25Bibliographically approved

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Sjöström, WilliamBotero, Carlos

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