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  • 1.
    Koli, Rohit R.
    et al.
    Shivaji Univ, Kolhapur, Maharashtra, India; Shivaji Univ, Kolhapur, Maharashtra, India.
    Phadatare, Manisha R.
    Mid Sweden University, Faculty of Science, Technology and Media, Department of Natural Sciences. DY Patil Univ, Kolhapur, Maharashtra, India.
    Sinha, Bhavesh B.
    Univ Mumbai, Mumbai, Maharashtra, India.
    Sakate, Deepak M.
    Shivaji Univ, Kolhapur, Maharashtra, India.
    Ghule, Anil V.
    Shivaji Univ, Kolhapur, Maharashtra, India.
    Ghodake, Gajanan S.
    Dongguk Univ Seoul, Goyang Si, Gyeonggi Do, India.
    Deshpande, Nishad G.
    Shivaji Univ, Dept Phys, Kolhapur, Maharashtra, India.
    Fulari, Vijay J.
    Shivaji Univ, Kolhapur, Maharashtra, India.
    Gram bean extract-mediated synthesis of Fe3O4 nanoparticles for tuning the magneto-structural properties that influence the hyperthermia performance2019In: Journal of the Taiwan Institute of Chemical Engineers / Elsevier, ISSN 1876-1070, E-ISSN 1876-1089, Vol. 95, p. 357-368Article in journal (Refereed)
    Abstract [en]

    A green synthesis of biocompatible magnetite (Fe3O4) nanoparticles (MNPs) using a combination of urea (U) and gram-bean extract (GBE, Cicer arietinum L.) is reported. The particle size of similar to 13 nm and highly stable magnetite phase is observed for GBE-U mediated MNPs. On the other hand, the MNPs synthesized using either U or GBE shows larger particle size and uneven size distribution. Interestingly, the sample with particle size similar to 13 nm shows optimum heat generation capacity (measured in specific absorption rate, i.e., SAR) near to the therapeutic temperature (43 degrees C) with least-variance. To investigate the influence of various factors such as variation in MNPs weight concentration (W-t), applied alternating magnetic field (AMF), saturation magnetization (M-s), magnetization rate (R-m), etc. on SAR, a multiple linear regression model (MLRM) is used. The study reveals a positive correlation of SAR with R-m, and AMF values while the negative correlation with M-s and W-t. Ultimately, the present green synthesis is the affordable approach for preparing stable and tiny MNPs. Moreover, MLRM is found to be a useful theoretical tool for understanding the influence of MNPs on hyperthermia performance. 

  • 2.
    Rastabi, Shahrzad Arshadi
    et al.
    Tarbiat Modares Univ, Tehran, Iran.
    Mamoory, Rasoul Sarraf
    Tarbiat Modares Univ, Tehran, Iran.
    Dabir, Fatemeh
    Niroo Res Inst, Tehran, Iran.
    Blomquist, Nicklas
    Mid Sweden University, Faculty of Science, Technology and Media, Department of Natural Sciences.
    Phadatare, Manisha R.
    Mid Sweden University, Faculty of Science, Technology and Media, Department of Natural Sciences.
    Olin, Håkan
    Mid Sweden University, Faculty of Science, Technology and Media, Department of Natural Sciences.
    Synthesis of NiMoO4/3D-rGO Nanocomposite in Alkaline Environments for Supercapacitor Electrodes2019In: Crystals, ISSN 2073-4352, Vol. 9, no 1, article id 31Article in journal (Refereed)
    Abstract [en]

    Although Graphene oxide (GO)-based materials is known as a favorable candidate for supercapacitors, its conductivity needs to be increased. Therefore, this study aimed to investigate the performance of GO-based supercapicitor with new methods. In this work, an ammonia solution has been used to remove the oxygen functional groups of GO. In addition, a facile precipitation method was performed to synthesis a NiMoO4/3D-rGO electrode with purpose of using synergistic effects of rGO conductivity properties as well as NiMoO4 pseudocapacitive behavior. The phase structure, chemical bands and morphology of the synthesized powders were investigated by X-ray diffraction (XRD), Raman spectroscopy, and field emission secondary electron microscopy (FE-SEM). The electrochemical results showed that the NiMoO4/3D-rGO(II) electrode, where ammonia has been used during the synthesis, has a capacitive performance of 932 Fg(-1). This is higher capacitance than NiMoO4/3D-rGO(I) without using ammonia. Furthermore, the NiMoO4/3D-rGO(II) electrode exhibited a power density of up to 17.5 kW kg(-1) and an energy density of 32.36 Wh kg(-1). These results showed that ammonia addition has increased the conductivity of rGO sheets, and thus it can be suggested as a new technique to improve the capacitance.

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