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Material Development for Electron Beam-based Powder Bed Fusion
Mid Sweden University, Faculty of Science, Technology and Media, Department of Engineering, Mathematics, and Science Education (2023-). (STRC)ORCID iD: 0000-0003-3218-875X
2024 (English)Licentiate thesis, comprehensive summary (Other academic)
Sustainable development
Hållbar utveckling
Abstract [en]

Electron beam powder bed fusion (PBF-EB) is an additivemanufacturing (AM) method based on layer-by-layer melting of apowder bed. The technology is industrialized in certain applicationsbut still considered as immature and is not as widely used as laserbeam-based systems (PBF-LB). PBF-EB can offer several benefits overPBF-LB such as process cleanliness, thermal efficiency, fast beam speed,higher power and energy transfer, low residual stresses in built partsand a good signal environment for process monitoring. This can beadded on top of the general benefits of AM such as geometricalfreedom, manufacturing efficiency, easy design revisions, short leadtimes and so on. This suggests that PBF-EB holds potential as atechnology for the sustainable production of materials andcomponents. This thesis investigates how PBF-EB can be furtherdeveloped to create new and unique materials features. This isachieved by introducing innovative methods for material processingand by further developing the PBF-EB process itself. The thesisintroduces a charge-free heating method for PBF-EB and the resultssuggest an enhanced processability of difficult-to-process materialsand powders. A method for building multi-materials in PBF-EB isintroduced and demonstrated by the manufacturing of direct andlamellar transitions between different alloys. Methods for processmonitoring and powder bed resistivity evaluation are proposed andxiidemonstrated. It is concluded that the results presented in this thesisenabled new PBF-EB processing modes, increased the knowledge ofthe process, and introduced a new material group by demonstratingthat ceramics can be processed at high temperatures (~1600C).

Place, publisher, year, edition, pages
Sundsvall: Mid Sweden University , 2024. , p. 109
Series
Mid Sweden University licentiate thesis, ISSN 1652-8948 ; 202
Keywords [en]
Additive manufacturing, Electron beam, Powder bed fusion, EBM, PBF-EB, PBF-EB/M, PBF-EB/C, Process development, Material development, Ti-6Al-4V, 316L, V4E, Al2O3
National Category
Mechanical Engineering
Identifiers
URN: urn:nbn:se:miun:diva-50762ISBN: 978-91-89786-54-7 (print)OAI: oai:DiVA.org:miun-50762DiVA, id: diva2:1840746
Presentation
2024-03-26, Q221, Akademigatan 1, Östersund, 09:00 (English)
Opponent
Supervisors
Note

Vid tidpunkten för framläggningen av avhandlingen var följande delarbeten opublicerade: delarbete 2 och delarbete 4 (inskickat).

At the time of the defence the following papers were unpublished: paper 2 and paper 4 (submitted).

Available from: 2024-02-27 Created: 2024-02-26 Last updated: 2024-03-05Bibliographically approved
List of papers
1. Near-infrared radiation: A promising heating method for powder bed fusion
Open this publication in new window or tab >>Near-infrared radiation: A promising heating method for powder bed fusion
2024 (English)In: Materials and Manufacturing Processes, ISSN 1042-6914, E-ISSN 1532-2475, Vol. 39, no 3, p. 320-328Article in journal (Refereed) Published
Abstract [en]

Metal additive manufacturing technologies, such as electron beam powder bed fusion (PBF-EB), rely on layer heating to overcome the so-called “smoke” phenomenon. When scaled up for industrial manufacturing, PBF-EB becomes less productive due to the lengthy preheating process. Currently, only the electron beam (EB) is used for preheating in PBF-EB, resulting in increased manufacturing times, energy consumption, and in some cases limiting the applicability of the technology. In this study, a new preheating approach is suggested that incorporates a near-infrared radiation (NIR) emitter inside an PBF-EB system. The NIR unit eliminates the need for EB heating, reducing build time and powder charging. Successful builds using 316 L and Ti6Al4V precursor powders validate the feasibility of the proposed approach. The produced samples exhibit similar properties to those obtained by the standard PBF-EB process. The introduction of NIR technology also reduced build cost and increased the service intervals of the electron gun. 

Place, publisher, year, edition, pages
Informa UK Limited, 2024
Keywords
316L, additive, beam, Electron, infrared, manufacturing, Ti6Al4V
National Category
Materials Engineering
Identifiers
urn:nbn:se:miun:diva-48165 (URN)10.1080/10426914.2023.2195910 (DOI)000961192700001 ()2-s2.0-85152071465 (Scopus ID)
Available from: 2023-04-19 Created: 2023-04-19 Last updated: 2024-02-27Bibliographically approved
2. Process developments in Electron Beam Powder Bed Fusion enabled by Near-Infrared Radiation
Open this publication in new window or tab >>Process developments in Electron Beam Powder Bed Fusion enabled by Near-Infrared Radiation
2024 (English)In: Journal of Manufacturing and Materials Processing, ISSN 2504-4494, Vol. 8, no 5, article id 211Article in journal (Refereed) Published
Abstract [en]

The use of an electron beam (EB) as a heating source in EB-based powder bed fusion (PBF-EB) has several limitations, such as reduced powder recyclability, short machine service intervals, difficulties with heating large areas and the limited processability of charge-sensitive powders. Near-infrared (NIR) heating was recently introduced as a feasible replacement and/or complement to EB heating in PBF-EB. This work further investigates the feasibility of using NIR to eliminate the need for a build platform as well as to enable easier repairing of parts in PBF-EB. NIR-assisted Ti-6Al-4V builds were successfully carried out by starting from a loose powder bed without using a build platform. The results do not only confirm that it is possible to eliminate the build platform by the aid of NIR, but also that it can be beneficial for the process cleanliness and improve the surface quality of built parts. Furthermore, a 430 stainless-steel (SS) component could be repaired by positioning it in a loose 316L SS powder bed using a fully NIR-heated PBF-EB process.

Place, publisher, year, edition, pages
MDPI AG, 2024
Keywords
electron beam, powder bed fusion, near-infrared heating, process manipulation, additive manufacturing, 316L, stainless steel, Ti-6Al-4V
National Category
Other Materials Engineering
Identifiers
urn:nbn:se:miun:diva-50772 (URN)10.3390/jmmp8050211 (DOI)001340929300001 ()2-s2.0-85207685253 (Scopus ID)
Available from: 2024-11-12 Created: 2024-02-27 Last updated: 2024-11-12Bibliographically approved
3. PBF-EB For Manufacturing Of 3D Metal-Metal Multi Material Assemblies
Open this publication in new window or tab >>PBF-EB For Manufacturing Of 3D Metal-Metal Multi Material Assemblies
Show others...
2023 (English)In: Euro Powder Metallurgy 2023 Congress and Exhibition, PM 2023, European Powder Metallurgy Association , 2023Conference paper, Published paper (Refereed)
Abstract [en]

Most Powder Bed Fusion (PBF) methods for the Additive Manufacturing (AM) of metals are based on the melting of powder of one specific metallic material; either of pure-elemental or pre-alloyed composition. Although the potential to build components from different materials in AM has recently gained a lot of attention, it is still not feasible in the current metal PBF systems. In the specific case of Electron beam- based PBF (PBF-EB), it is possible to precisely control the beam parameters in each site of the build area, which opens great possibilities for adaptive processes that allows melting powders of different nature in the same build. In this investigation, different steel-based and Ti6Al4V alloy powders are used to create metal-metal assemblies. By steering the fetching of two powders loaded in different hoppers it was possible to build different metal-metal assemblies. The microstructure and mechanical properties of the final materials were evaluated. 

Place, publisher, year, edition, pages
European Powder Metallurgy Association, 2023
National Category
Materials Engineering
Identifiers
urn:nbn:se:miun:diva-50225 (URN)10.59499/EP235735468 (DOI)2-s2.0-85180376917 (Scopus ID)
Conference
Euro Powder Metallurgy 2023 Congress and Exhibition, PM 2023
Available from: 2024-01-08 Created: 2024-01-08 Last updated: 2024-02-27Bibliographically approved
4. Melting ceramic Al2O3 powder by electron beam powder bed fusion
Open this publication in new window or tab >>Melting ceramic Al2O3 powder by electron beam powder bed fusion
2024 (English)In: Progress in Additive Manufacturing, ISSN 2363-9512, Vol. 9, p. 1523-1535Article in journal (Refereed) Published
Abstract [en]

Electron beam powder bed fusion (PBF-EB) is a known metal additive manufacturing (AM) technology. Processing non-conducting powders such as ceramics has so far been considered as not feasible because of the inherent problems with Coulomb repulsion due to insufficient electrical conductivity. In this study, a method for functionalizing ceramic powder is proposed where particles are electroless coated by a ~ 1 µm Ni layer to decrease the surface resistivity. The feasibility of the suggested approach is tested on Al2O3 powder, and the results show that the coated ceramic powder has a decreased surface resistivity, which enables processing by PBF-EB. Heating and melting parameters were investigated and samples were manufactured at ~ 1600 °C. Sintered and melted powders were analyzed by microscopy and micromechanically tested by nanoindentation. Calculations, visual observation and SEM–EDX suggest that the Ni coating is evaporated during the process, which suggests that the process could be feasible for the manufacturing of pure ceramic parts.

Place, publisher, year, edition, pages
Springer, 2024
National Category
Other Materials Engineering
Identifiers
urn:nbn:se:miun:diva-50773 (URN)10.1007/s40964-024-00601-4 (DOI)2-s2.0-85189612765 (Scopus ID)
Available from: 2024-11-12 Created: 2024-02-27 Last updated: 2024-11-12Bibliographically approved

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