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Electron beam powder bed fusion processing of 2507 super duplex stainless steel. as-built phase composition and microstructural properties
Mid Sweden University, Faculty of Science, Technology and Media, Department of Engineering, Mathematics, and Science Education (2023-). (Sports Tech Research Centre)ORCID iD: 0000-0002-2543-2809
Mid Sweden University, Faculty of Science, Technology and Media, Department of Engineering, Mathematics, and Science Education (2023-). (Sports Tech Research Centre)
Mid Sweden University, Faculty of Science, Technology and Media, Department of Engineering, Mathematics, and Science Education (2023-). (Sports Tech Research Centre)ORCID iD: 0000-0001-5954-5898
2023 (English)In: Journal of Materials Research and Technology, ISSN 2238-7854, E-ISSN 2214-0697, Vol. 24, p. 6473-6483Article in journal (Refereed) Published
Abstract [en]

This study focuses on adapting the Electron Beam Powder Bed Fusion (E-PBF) process for the manufacturing of parts from 2507 super duplex stainless steel, combining high strength and corrosion resistance, therefore presenting an interesting choice for E-PBF implementation. Samples manufactured using four sets of process parameters were characterized by scanning electron microscopy, tensile testing, X-ray diffraction analysis, energy dispersive X-ray spectroscopy and nanoindentation. The different E-PBF process temperatures investigated had the strongest influence on the phase characteristics and the resulting microstructure. The processability of the material was good, and high productivity rates were achieved, indicating good suitability for industrial transfer.

Place, publisher, year, edition, pages
Elsevier, 2023. Vol. 24, p. 6473-6483
Keywords [en]
1.4410, 2507, Additive manufacturing, Electron beam powder bed fusion, Nanoindentation, Stainless steel
National Category
Metallurgy and Metallic Materials
Identifiers
URN: urn:nbn:se:miun:diva-48320DOI: 10.1016/j.jmrt.2023.04.230ISI: 001026745000001Scopus ID: 2-s2.0-85156260914OAI: oai:DiVA.org:miun-48320DiVA, id: diva2:1757192
Available from: 2023-05-16 Created: 2023-05-16 Last updated: 2024-09-02Bibliographically approved
In thesis
1. Electron beam powder bed fusion processing of stainless steels
Open this publication in new window or tab >>Electron beam powder bed fusion processing of stainless steels
2023 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

Additive manufacturing (AM) is still a relatively new technology. In contrast to traditional machining where material is removed from a blank, AM is used to fuse a feedstock material into complex shapes, layer by layer, starting from an empty workspace. AM enables the manufacture of complex part geometries and part variations with little to no extra manufacturing cost. Manufacturing of geometries which was not previously possible, are now available as design options such as bent internal channels, intricate lattice structures and designed surface porosity - all of which can be produced repeatably. Electron beam powder bed fusion (PBF-EB) is an AM method in which an electron beam is used to process a fine-grained powder into parts. Since its conception, PBF-EB has been hampered by the number of materials available for processing. The aim of this thesis is to explore the possibilities for processing stainless steels using PBF-EB. The work is focused on the development of parameters for efficient processing with the aim of achieving high-density as-built materials and an understanding of the relationship between process parameters and the resulting microstructure and other quality aspects of the parts. Two stainless steel powders, 316LN (austenitic) and super duplex 2507 (austenitic / ferritic), are processed via a wide range of process parameters into solid parts using various melting strategies. Density, microstructural features, and mechanical properties are evaluated and assessed before selecting a set of parameters that produce high-quality parts at a high processing rate. This work concludes that stainless steels are well suited for PBF-EB processing, with a wide processing window. The studies also show that the material properties are highly influenced by the processing parameters used. In the case of super duplex stainless steel 2507 the built parts require post-build heat treatment to achieve the desired microstructure, phase-composition and tensile properties, while 316LN can to a larger extent be used as-built, provided that proper build preparation and processing parameters are used.

Place, publisher, year, edition, pages
Östersund: Mid Sweden University, 2023. p. 85
Series
Mid Sweden University doctoral thesis, ISSN 1652-893X ; 396
Keywords
Additive manufacturing, Electron beam powder bed fusion, PBF-EB, Stainless steel, Mechanical properties, Micro-structure, Nanoindentation
National Category
Mechanical Engineering
Identifiers
urn:nbn:se:miun:diva-49338 (URN)978-91-89786-31-8 (ISBN)
Public defence
2023-10-17, Q221, Akademigatan 1, 83140 Östersund, Östersund, 09:00 (English)
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Supervisors
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Knowledge FoundationInterreg
Note

Vid tidpunkten för disputationen var följande delarbeten opublicerade: delarbete 5 under granskning och delarbete 6 manuskript.

At the time of the doctoral defence the following papers were unpublished: paper 5 under review and paper 6 in manuscript.

Available from: 2023-09-22 Created: 2023-09-19 Last updated: 2023-09-19Bibliographically approved

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Roos, StefanBotero, CarlosRännar, Lars-Erik

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